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| CLP Pesticide Standards |
The USEPA Contract Laboratory Program (CLP) is a contract trhough which the USEPA may retain analytical services. The CLP contracts contain detailed operating procedures to be followed by those laboratories which are awarded the contracts. The methods arederived from SW-846 and the USEPA-Office of Research and Development. Many state and federal agencies look to the CLP methods for guidance in terms of analytical parameters as a result of the large body of performance data which has been generated tovalidate the CLP methods.
The CLP Pesticide analysis method, from the OLM04.1, is an analytical method which utilizes a methylene chloride extraction of aqueous sample or a methylene chloride: acetone extraction of 30 grams of solid sample,concentrated after clean-up to 10 mL and a gas chromatograph equipped with a packed column to perform the separation of pesticides and PCB's. To detect the GC eluant, an ECD is used.
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1000 TIMES HIGH POINT CONCENTR |
| Compound | µg/mL | | Aldrin | 80 |
| beta-BHC | 80 |
| alpha-Chlordane | 80 |
| p,p'-DDE | 160 |
| Decachlorobiphenyl | 160 |
| delta-BHC | 80 |
| Endosulfan II | 160 |
| Endosulfan sulfate | 160 |
| Endrin aldehyde | 160 |
| Endrin ketone | 160 |
| gamma-Chlordane | 80 |
| Heptachlor epoxide | 80 |
| 2,4,5,6-Tetrachloro-m-xylene | 80 |
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 | 1.2 mL @ 80 µg/ml in HEXTOL Catalog#: CLPP-B90-1000 | $64.00 | |
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 | 1.2 mL @ 160 µg/ml in HEXTOL Catalog#: CLPP-B90-1000 | $64.00 | |
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1000 TIMES LOW POINT CONCENTRA |
| Compound | µg/mL | | alpha-BHC | 5 |
| p,p'-DDD | 10 |
| Decachlorobiphenyl | 10 |
| Dieldrin | 10 |
| p,p'-DDT | 10 |
| Endosulfan I | 5 |
| Endrin | 10 |
| gamma-BHC | 5 |
| Heptachlor | 5 |
| Methoxychlor | 50 |
| 2,4,5,6-Tetrachloro-m-xylene | 5 |
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 | 1.2 mL @ 5 µg/ml in ISOOCT Catalog#: CLPP-A90-S | $37.00 | |
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 | 1.2 mL @ 10 µg/ml in ISOOCT Catalog#: CLPP-A90-S | $37.00 | |
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 | 1.2 mL @ 50 µg/ml in ISOOCT Catalog#: CLPP-A90-S | $37.00 | |
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3/90-SOW MATRIX SPIKE |
| Compound | µg/mL | | Aldrin | 0.5 |
| Aldrin | 0.5 |
| Dieldrin | 2 |
| p,p'-DDT | 2 |
| Endrin | 2 |
| gamma-BHC | 0.5 |
| Heptachlor | 0.5 |
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 | 25 mL @ 0.5 ng/ml in METH Catalog#: CLPP-MS90-25 | $44.00 | |
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 | 25 mL @ 2 µg/ml in METH Catalog#: CLPP-MS90-25 | $44.00 | |
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 | 25 mL @ 2 ng/ml in METH Catalog#: CLPP-MS90-25 | $44.00 | |
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 | 50 mL @ 0.5 µg/ml in METH Catalog#: CLPP-MS90-50 | $65.00 | |
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 | 50 mL @ 0.5 ng/ml in METH Catalog#: CLPP-MS90-50 | $65.00 | |
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 | 50 mL @ 2 µg/ml in METH Catalog#: CLPP-MS90-50 | $65.00 | |
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 | 50 mL @ 2 ng/ml in METH Catalog#: CLPP-MS90-50 | $65.00 | |
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3/90-SOW SURROGATE SPIKE |
Decachlorobiphenyl
2,4,5,6-Tetrachloro-m-xylene
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 | 100 mL @ 0.2 µg/ml in AC Catalog#: CLPP-SS90-100 | $52.00 |  |
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 | 100 mL @ 0.2 ng/ml in AC Catalog#: CLPP-SS90-100 | $52.00 |  |
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 | 100 mL @ 0.2 µg/ml in Acetone - Tinted Indicator Catalog#: CLPP-SS90-100-TI | $57.00 | |
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 | 100 mL @ 0.2 ng/ml in Acetone - Tinted Indicator Catalog#: CLPP-SS90-100-TI | $57.00 | |
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3/90=SOW MATRIX SPIKE |
| Compound | µg/mL | | Aldrin | 0.5 |
| Dieldrin | 2 |
| p,p'-DDT | 2 |
| Endrin | 2 |
| gamma-BHC | 0.5 |
| Heptachlor | 0.5 |
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 | 100 mL @ 0.5 µg/ml in METH Catalog#: CLPP-MS90-100 | $110.00 | |
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 | 100 mL @ 0.5 ng/ml in METH Catalog#: CLPP-MS90-100 | $110.00 | |
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 | 100 mL @ 2 µg/ml in METH Catalog#: CLPP-MS90-100 | $110.00 | |
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 | 100 mL @ 2 ng/ml in METH Catalog#: CLPP-MS90-100 | $110.00 | |
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90-SOW MATRIX SPIKE |
| Compound | µg/mL | | Aldrin | 50 |
| Dieldrin | 200 |
| p,p'-DDT | 200 |
| Endrin | 200 |
| gamma-BHC | 50 |
| Heptachlor | 50 |
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 | 1.2 mL @ 50 µg/ml in METH Catalog#: CLPP-MS90 | $27.00 | |
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 | 1.2 mL @ 200 µg/ml in METH Catalog#: CLPP-MS90 | $27.00 | |
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91-SOW SURR SPIKE |
| Compound | µg/mL | | Decachlorobiphenyl | 200 |
| 2,4,5,6-Tetrachloro-m-xylene | 100 |
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