500 Series Method 501 Method 502.1 Method 502.2 Method 503.1 Method 504/504.1 Method 505 Method 506 Method 507 Method 508 Method 508.1 Method 508A Method 515.1 Method 515.2 Method 524.2 Method 525.2 Method 531.1 Method 547 Method 548 Method 548.1 Method 549.1 Method 550/550.1 Method 551.1 Method 552 Method 552.1 Method 552.2 600 Series Method 601 Method 602 Method 603 Method 604 Method 605 Method 606 Method 607 Method 608 Method 608.1 Method 608.2 Method 609 Method 610 Method 611 Method 612 Method 614 Method 614.1 Method 615 Method 617 Method 618 Method 619 Method 620 Method 622 Method 624 Method 625 Method 627-645 Method 632 8000 Series Method 8010A Method 8010B Method 8011 Method 8015A Method 8015B Method 8020/8020A Method 8021/8021A/8021B Method 8030 Method 8031 Method 8032A Method 8033 Method 8040 Method 8041 Method 8060 Method 8061 Method 8070 Method 8080A/8081A Method 8082 Method 8090 Method 8091 Method 8100 Method 8110 Method 8111 Methods 8120/8120A/8121 Methods 8140/8141 Methods 8150A/8150B/8151 Method 8240B Method 8260B Method 8270C Method 8310 CLP Semivolatile Standards CLP Semivolatile Standards CLP Pesticide Standards CLP Pesticide Standards CLP Volatile Standards CLP Volatile Standards TCLP - Method 1311 TCLP - Method 1311 Petrochemical/LUST Standards Petrochemical/LUST Standards Internal Standards Internal Standards / Surroga... New Tinted Indicator Surroga... Single-Component Standards Columns CA-1 (Methyl Silicone) CA-1701 (14% Cyano Silicone) CA-5 5% (Phenyl Silicone) CA-502.2 CA-FFAP (Acid Modified PEG) CA-Wax (Polyethylene Glycol) Intermediate Polarity Guard ... Non-Polar Guard Columns Polar Guard Columns Request a Custom Column Column Installation Tips QC Samples QC Samples for WP - Inorgani... QC Samples for WP - Organic QC Samples for WS - Inorgani... QC Samples for WS - Organic

Table of Contents  CLP Pesticide Standards The USEPA Contract Laboratory Program (CLP) is a contract trhough which the USEPA may retain analytical services. The CLP contracts contain detailed operating procedures to be followed by those laboratories which are awarded the contracts. The methods arederived from SW-846 and the USEPA-Office of Research and Development. Many state and federal agencies look to the CLP methods for guidance in terms of analytical parameters as a result of the large body of performance data which has been generated tovalidate the CLP methods. The CLP Pesticide analysis method, from the OLM04.1, is an analytical method which utilizes a methylene chloride extraction of aqueous sample or a methylene chloride: acetone extraction of 30 grams of solid sample,concentrated after clean-up to 10 mL and a gas chromatograph equipped with a packed column to perform the separation of pesticides and PCB's. To detect the GC eluant, an ECD is used.  1000 TIMES HIGH POINT CONCENTR Compound µg/mL Aldrin 80 beta-BHC 80 alpha-Chlordane 80 p,p'-DDE 160 Decachlorobiphenyl 160 delta-BHC 80 Endosulfan II 160 Endosulfan sulfate 160 Endrin aldehyde 160 Endrin ketone 160 gamma-Chlordane 80 Heptachlor epoxide 80 2,4,5,6-Tetrachloro-m-xylene 80           1.2 mL @ 80 µg/ml in HEXTOL   Catalog#: CLPP-B90-1000  $64.00           1.2 mL @ 160 µg/ml in HEXTOL   Catalog#: CLPP-B90-1000  $64.00     1000 TIMES LOW POINT CONCENTRA Compound µg/mL alpha-BHC 5 p,p'-DDD 10 Decachlorobiphenyl 10 Dieldrin 10 p,p'-DDT 10 Endosulfan I 5 Endrin 10 gamma-BHC 5 Heptachlor 5 Methoxychlor 50 2,4,5,6-Tetrachloro-m-xylene 5           1.2 mL @ 5 µg/ml in ISOOCT   Catalog#: CLPP-A90-S  $37.00           1.2 mL @ 10 µg/ml in ISOOCT   Catalog#: CLPP-A90-S  $37.00           1.2 mL @ 50 µg/ml in ISOOCT   Catalog#: CLPP-A90-S  $37.00     3/90-SOW MATRIX SPIKE Compound µg/mL Aldrin 0.5 Aldrin 0.5 Dieldrin 2 p,p'-DDT 2 Endrin 2 gamma-BHC 0.5 Heptachlor 0.5           25 mL @ 0.5 ng/ml in METH   Catalog#: CLPP-MS90-25  $44.00           25 mL @ 2 µg/ml in METH   Catalog#: CLPP-MS90-25  $44.00           25 mL @ 2 ng/ml in METH   Catalog#: CLPP-MS90-25  $44.00           50 mL @ 0.5 µg/ml in METH   Catalog#: CLPP-MS90-50  $65.00           50 mL @ 0.5 ng/ml in METH   Catalog#: CLPP-MS90-50  $65.00           50 mL @ 2 µg/ml in METH   Catalog#: CLPP-MS90-50  $65.00           50 mL @ 2 ng/ml in METH   Catalog#: CLPP-MS90-50  $65.00     3/90-SOW SURROGATE SPIKE Decachlorobiphenyl 2,4,5,6-Tetrachloro-m-xylene           100 mL @ 0.2 µg/ml in AC   Catalog#: CLPP-SS90-100  $52.00           100 mL @ 0.2 ng/ml in AC   Catalog#: CLPP-SS90-100  $52.00           100 mL @ 0.2 µg/ml in Acetone - Tinted Indicator   Catalog#: CLPP-SS90-100-TI  $57.00           100 mL @ 0.2 ng/ml in Acetone - Tinted Indicator   Catalog#: CLPP-SS90-100-TI  $57.00     3/90=SOW MATRIX SPIKE Compound µg/mL Aldrin 0.5 Dieldrin 2 p,p'-DDT 2 Endrin 2 gamma-BHC 0.5 Heptachlor 0.5           100 mL @ 0.5 µg/ml in METH   Catalog#: CLPP-MS90-100  $110.00           100 mL @ 0.5 ng/ml in METH   Catalog#: CLPP-MS90-100  $110.00           100 mL @ 2 µg/ml in METH   Catalog#: CLPP-MS90-100  $110.00           100 mL @ 2 ng/ml in METH   Catalog#: CLPP-MS90-100  $110.00     90-SOW MATRIX SPIKE Compound µg/mL Aldrin 50 Dieldrin 200 p,p'-DDT 200 Endrin 200 gamma-BHC 50 Heptachlor 50           1.2 mL @ 50 µg/ml in METH   Catalog#: CLPP-MS90  $27.00           1.2 mL @ 200 µg/ml in METH   Catalog#: CLPP-MS90  $27.00     91-SOW SURR SPIKE Compound µg/mL Decachlorobiphenyl 200 2,4,5,6-Tetrachloro-m-xylene 100           25 mL @ 100 µg/ml in AC   Catalog#: CLPP-S91  $16.00           25 mL @ 200 µg/ml in AC   Catalog#: CLPP-S91  $16.00           1.2 mL @ 100 µg/ml in Acetone - Tinted Indicator   Catalog#: CLPP-S91-TI  $21.00           1.2 mL @ 200 µg/ml in Acetone - Tinted Indicator   Catalog#: CLPP-S91-TI  $21.00     FLORISIL CARTRIDGE CHECK SOLUT 2,4,5-Trichlorophenol           1.2 mL @ 200 µg/ml in AC   Catalog#: FLO-CAL  $16.00     GEL PERMEATION CLEAN-UP CALIBR Compound µg/mL bis(2-Ethylhexyl)phthalate 5 bis(2-Ethylhexyl)phthalate 10 Corn Oil 250 Methoxychlor 1 Methoxychlor 2 Perylene 0.2 Sulfur 0.8           5.2 mL @ 0.2 mg/ml in MC   Catalog#: GPC-CAL-91  $27.00           5.2 mL @ 0.8 mg/ml in MC   Catalog#: GPC-CAL-91  $27.00           5.2 mL @ 2 mg/ml in MC   Catalog#: GPC-CAL-91  $27.00           5.2 mL @ 10 mg/ml in MC   Catalog#: GPC-CAL-91  $27.00           5.2 mL @ 250 mg/ml in MC   Catalog#: GPC-CAL-91  $27.00           5.2 mL @ 0.2 mg/ml in MC   Catalog#: GPC-CAL-93  $27.00           5.2 mL @ 0.8 mg/ml in MC   Catalog#: GPC-CAL-93  $27.00           5.2 mL @ 1 mg/ml in MC   Catalog#: GPC-CAL-93  $27.00           5.2 mL @ 5 mg/ml in MC   Catalog#: GPC-CAL-93  $27.00           5.2 mL @ 250 mg/ml in MC   Catalog#: GPC-CAL-93  $27.00     IND. AROCLORS Aroclor 1242 Aroclor 1254 Aroclor 1016 Aroclor 1221 Arochlor 1232 Aroclor 1260 Aroclor 1262 Aroclor 1268           1.2 mL @ 1000 µg/ml in HEX   Catalog#: PCB-1016H  $27.00           1.2 mL @ 1000 µg/ml in HEX   Catalog#: PCB-1221H  $28.00           1.2 mL @ 1000 µg/ml in HEX   Catalog#: PCB-1232H  $27.00           1.2 mL @ 1000 µg/ml in HEX   Catalog#: PCB-1242H  $27.00           1.2 mL @ 200 µg/ml in HEX   Catalog#: PCB-1254  $16.00           1.2 mL @ 200 µg/ml in HEX   Catalog#: PCB-1260  $16.00           1.2 mL @ 200 µg/ml in HEX   Catalog#: PCB-1262  $15.00           1.2 mL @ 200 µg/ml in HEX   Catalog#: PCB-1268  $16.00     IND. STD MIX A For 2-88 SOW Compound µg/mL Aldrin 5 Dieldrin 10 p,p'-DDT 20 Endosulfan I 10 Endosulfan II 20 Endrin aldehyde 25 gamma-BHC 5 Heptachlor 10 Heptachlor epoxide 10 Methoxychlor 100           10 mL @ 5 µg/ml in HEXTOL   Catalog#: CLPP-A88  $21.00           10 mL @ 10 µg/ml in HEXTOL   Catalog#: CLPP-A88  $21.00           10 mL @ 20 µg/ml in HEXTOL   Catalog#: CLPP-A88  $21.00           10 mL @ 25 µg/ml in HEXTOL   Catalog#: CLPP-A88  $21.00           10 mL @ 100 µg/ml in HEXTOL   Catalog#: CLPP-A88  $21.00     IND. STD MIX A For 3-90 & 7-91 Compound µg/mL alpha-BHC 5 alpha-BHC 80 p,p'-DDD 10 p,p'-DDD 160 Decachlorobiphenyl 160 Dieldrin 10 Dieldrin 160 p,p'-DDT 10 p,p'-DDT 160 Endosulfan I 5 Endosulfan I 80 Endrin 10 Endrin 160 gamma-BHC 5 gamma-BHC 80 Heptachlor 5 Heptachlor 80 Methoxychlor 50 Methoxychlor 800 2,4,5,6-Tetrachloro-m-xylene 80           1.2 mL @ 5 µg/ml in HEXTOL   Catalog#: CLPP-A90  $21.00           1.2 mL @ 10 µg/ml in HEXTOL   Catalog#: CLPP-A90  $21.00           1.2 mL @ 50 µg/ml in HEXTOL   Catalog#: CLPP-A90  $21.00           1.2 mL @ 80 µg/ml in ISOOCT   Catalog#: CLPP-A90-1000  $64.00           1.2 mL @ 160 µg/ml in ISOOCT   Catalog#: CLPP-A90-1000  $64.00           1.2 mL @ 800 µg/ml in ISOOCT   Catalog#: CLPP-A90-1000  $64.00     IND. STD MIX A For 7-91 SOW Compound µg/mL alpha-BHC 5 alpha-BHC 20 alpha-BHC 80 p,p'-DDD 10 p,p'-DDD 40 p,p'-DDD 160 Decachlorobiphenyl 10 Decachlorobiphenyl 40 Decachlorobiphenyl 160 Dieldrin 10 Dieldrin 40 Dieldrin 160 p,p'-DDT 10 p,p'-DDT 40 p,p'-DDT 160 Endosulfan I 5 Endosulfan I 20 Endosulfan I 80 Endrin 10 Endrin 40 Endrin 160 gamma-BHC 5 gamma-BHC 20 gamma-BHC 80 Heptachlor 5 Heptachlor 20 Heptachlor 80 Methoxychlor 50 Methoxychlor 200 Methoxychlor 800 2,4,5,6-Tetrachloro-m-xylene 5 2,4,5,6-Tetrachloro-m-xylene 20 2,4,5,6-Tetrachloro-m-xylene 80           1.2 mL @ 80 ng/ml in ISOOCT   Catalog#: CLPP-90-HA  $16.00           1.2 mL @ 160 ng/ml in ISOOCT   Catalog#: CLPP-90-HA  $16.00           1.2 mL @ 800 ng/ml in ISOOCT   Catalog#: CLPP-90-HA  $16.00           10 mL @ 5 ng/ml in ISOOCT   Catalog#: CLPP-90-LA  $16.00           10 mL @ 10 ng/ml in ISOOCT   Catalog#: CLPP-90-LA  $16.00           10 mL @ 50 ng/ml in ISOOCT   Catalog#: CLPP-90-LA  $16.00           1.2 mL @ 20 ng/ml in ISOOCT   Catalog#: CLPP-90-MA  $16.00           1.2 mL @ 40 ng/ml in ISOOCT   Catalog#: CLPP-90-MA  $16.00           1.2 mL @ 200 ng/ml in ISOOCT   Catalog#: CLPP-90-MA  $16.00     IND. STD MIX B For 2-88 SOW Compound µg/mL Aldrin 5 alpha-BHC 5 beta-BHC 10 alpha-Chlordane 10 p,p'-DDD 20 p,p'-DDE 10 delta-BHC 10 Endosulfan sulfate 20 Endrin 10 Endrin ketone 20 gamma-Chlordane 10           1.2 mL @ 5 µg/ml in HEXTOL   Catalog#: CLPP-B88  $21.00           1.2 mL @ 10 µg/ml in HEXTOL   Catalog#: CLPP-B88  $21.00           1.2 mL @ 20 µg/ml in HEXTOL   Catalog#: CLPP-B88  $21.00     IND. STD MIX B For 3-90 & 7-91 Compound µg/mL Aldrin 5 beta-BHC 5 alpha-Chlordane 5 p,p'-DDE 10 delta-BHC 5 Endosulfan II 10 Endosulfan sulfate 10 Endrin aldehyde 10 Endrin ketone 10 gamma-Chlordane 5 Heptachlor epoxide 5           10 mL @ 5 µg/ml in HEXTOL   Catalog#: CLPP-B90  $21.00           10 mL @ 10 µg/ml in HEXTOL   Catalog#: CLPP-B90  $21.00     IND. STD MIX B For 7-91 SOW Compound µg/mL Aldrin 5 Aldrin 5 Aldrin 20 Aldrin 80 beta-BHC 5 beta-BHC 5 beta-BHC 20 beta-BHC 80 alpha-Chlordane 5 alpha-Chlordane 5 alpha-Chlordane 20 alpha-Chlordane 80 p,p'-DDE 10 p,p'-DDE 10 p,p'-DDE 40 p,p'-DDE 160 Decachlorobiphenyl 10 Decachlorobiphenyl 1 Decachlorobiphenyl 40 Decachlorobiphenyl 160 delta-BHC 5 delta-BHC 5 delta-BHC 20 delta-BHC 80 Endosulfan II 10 Endosulfan II 10 Endosulfan II 40 Endosulfan II 160 Endosulfan sulfate 10 Endosulfan sulfate 10 Endosulfan sulfate 40 Endosulfan sulfate 160 Endrin aldehyde 10 Endrin aldehyde 10 Endrin aldehyde 40 Endrin aldehyde 160 Endrin ketone 10 Endrin ketone 10 Endrin ketone 40 Endrin ketone 160 gamma-Chlordane 5 gamma-Chlordane 5 gamma-Chlordane 20 gamma-Chlordane 80 Heptachlor epoxide 5 Heptachlor epoxide 5 Heptachlor epoxide 20 Heptachlor epoxide 80 2,4,5,6-Tetrachloro-m-xylene 5 2,4,5,6-Tetrachloro-m-xylene 5 2,4,5,6-Tetrachloro-m-xylene 20 2,4,5,6-Tetrachloro-m-xylene 80           1.2 mL @ 80 ng/ml in ISOOCT   Catalog#: CLPP-90-HB  $16.00           1.2 mL @ 160 ng/ml in ISOOCT   Catalog#: CLPP-90-HB  $16.00           1.2 mL @ 5 ng/ml in ISOOCT   Catalog#: CLPP-90-LB  $16.00           1.2 mL @ 10 ng/ml in ISOOCT   Catalog#: CLPP-90-LB  $16.00           1.2 mL @ 20 ng/ml in ISOOCT   Catalog#: CLPP-90-MB  $16.00           1.2 mL @ 40 ng/ml in ISOOCT   Catalog#: CLPP-90-MB  $16.00           1.2 mL @ 1 µg/ml in ISOOCT   Catalog#: CLPP-B90-S  $37.00           1.2 mL @ 5 µg/ml in ISOOCT   Catalog#: CLPP-B90-S  $37.00           1.2 mL @ 10 µg/ml in ISOOCT   Catalog#: CLPP-B90-S  $37.00     LOW-LEVEL CLP PEST Compound µg/mL p,p'-DDE 20 Dieldrin 20 Endosulfan sulfate 20 Endrin 20 gamma-BHC 10 gamma-Chlordane 10 Heptachlor epoxide 10           1.2 mL @ 10 µg/ml in AC   Catalog#: CLPP-LLA  $27.00           1.2 mL @ 20 µg/ml in AC   Catalog#: CLPP-LLA  $27.00     PERFORMANCE EVAL MIX Compound µg/mL alpha-BHC 1 beta-BHC 1 p,p'-DDT 10 Endrin 5 gamma-BHC 1 Methoxychlor 25           1.2 mL @ 1 µg/ml in HEXTOL   Catalog#: CLPP-PEM  $21.00           1.2 mL @ 5 µg/ml in HEXTOL   Catalog#: CLPP-PEM  $21.00           1.2 mL @ 10 µg/ml in HEXTOL   Catalog#: CLPP-PEM  $21.00           1.2 mL @ 25 µg/ml in HEXTOL   Catalog#: CLPP-PEM  $21.00     RADY-PREP 91-SOW MATRIX SPIKE Compound µg/mL Aldrin 0.5 Dieldrin 1 p,p'-DDT 1 Endrin 1 gamma-BHC 0.5 Heptachlor 0.5           100 mL @ 0.5 µg/ml in METH   Catalog#: CLPP-MS91-100  $111.00           100 mL @ 1 µg/ml in METH   Catalog#: CLPP-MS91-100  $111.00     READY-PREP 91-SOW SUR SPIKE Compound µg/mL Decachlorobiphenyl 0.2 2,4,5,6-Tetrachloro-m-xylene 0.1           25 mL @ 0.1 µg/ml in AC   Catalog#: CLPP-SS91-25  $19.00           25 mL @ 0.2 ng/ml in AC   Catalog#: CLPP-SS91-25  $19.00           25 mL @ 0.1 µg/ml in Acetone - Tinted Indicator   Catalog#: CLPP-SS91-25-TI  $24.00           25 mL @ 0.2 ng/ml in Acetone - Tinted Indicator   Catalog#: CLPP-SS91-25-TI  $24.00     READY-PREP 91-SOW SURROGATE SPIKE Compound µg/mL Decachlorobiphenyl 0.2 2,4,5,6-Tetrachloro-m-xylene 0.1           50 mL @ 0.1 µg/ml in AC   Catalog#: CLPP-SS91-50  $30.00           50 mL @ 0.2 ng/ml in AC   Catalog#: CLPP-SS91-50  $30.00           50 mL @ 0.1 µg/ml in Acetone - Tinted Indicator   Catalog#: CLPP-SS91-50-TI  $36.00           50 mL @ 0.2 ng/ml in Acetone - Tinted Indicator   Catalog#: CLPP-SS91-50-TI  $36.00     READY-PREP91-SOW MATRIX SPIKE Compound µg/mL Aldrin 0.5 Dieldrin 1 p,p'-DDT 1 Endrin 1 gamma-BHC 0.5 Heptachlor 0.5           25 mL @ 0.5 µg/ml in METH   Catalog#: CLPP-MS91-25  $45.00           25 mL @ 0.5 ng/ml in METH   Catalog#: CLPP-MS91-25  $45.00           25 mL @ 1 µg/ml in METH   Catalog#: CLPP-MS91-25  $45.00           25 mL @ 1 ng/ml in METH   Catalog#: CLPP-MS91-25  $45.00     Toxaphene Toxaphene             10 mL @ 1000 µg/ml in HEX   Catalog#: S-3535  $20.00