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 Method 552.1
The USEPA method 552.1 utilizes a liquid-solid extraction to determine haloacetic acids, disinfection by-products an dthe chlorinated herbicide, Dalapon. The sample is extracted with a miniature anion exchange column and the analytes are methylateddirectly in the eluent using acidic acidic methanol instead of diazomethane. A gas chromatograph equipped with a capillary column is used to perform the separation of methyl-haloacetates and anisoles. To detect the GC eluant, an ECD (Electron capture)detector is used.
 

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