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| Table of Contents |
| < Method 552 |
Method 552.2 > |
| Method 552.1 |
The USEPA method 552.1 utilizes a liquid-solid extraction to determine haloacetic acids, disinfection by-products an dthe chlorinated herbicide, Dalapon. The sample is extracted with a miniature anion exchange column and the analytes are methylateddirectly in the eluent using acidic acidic methanol instead of diazomethane. A gas chromatograph equipped with a capillary column is used to perform the separation of methyl-haloacetates and anisoles. To detect the GC eluant, an ECD (Electron capture)detector is used.
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1,2,3-Trichloropropane |
1,2,3-Trichloropropane
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 | 1.2 mL @ 1000 µg/ml in METH-P&T Catalog#: S-3665 | $20.00 | |
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2,3-Dibromopropionic Acid |
2,3-Dibromopropionic acid
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 | 1.2 mL @ 1000 µg/ml in METH-P&T Catalog#: S-3895 | $35.00 |  |
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FREE ACIDS |
Bromoacetic acid
Bromochloroacetic acid
Chloroacetic acid
Dalapon
| Dibromoacetic acid
Dichloroacetic acid
Trichloroacetic acid
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 | 1.2 mL @ 200 µg/ml in MTBE Catalog#: 5521-A | $53.00 | |
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 | 1.2 ML X 4 PACK Catalog#: 5521-A-4 | $165.00 | |
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METH 552.1 METHYL ESTERS |
| Compound | µg/mL | | Dalapon | 200 |
| Methyl-Bromoacetate | 200 |
| Methyl-bromochloroacetate | 200 |
| Methyl-Chloroacetate | 300 |
| | Compound | µg/mL | | Methyl-Dibromoacetate | 100 |
| Methyl-Dichloroacetate | 300 |
| Methyl-Trichloroacetate | 100 |
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 | 1.2 mL @ 100 µg/ml in MTBE Catalog#: 5521-MEO | $37.00 | |
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 | 1.2 mL @ 200 µg/ml in MTBE Catalog#: 5521-MEO | $37.00 | |
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 | 1.2 mL @ 300 µg/ml in MTBE Catalog#: 5521-MEO | $37.00 | |
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Methyl-2-Bromopropionate |
Methyl-2-bromopropionate
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 | 1.2 mL @ 1000 µg/ml in MTBE Catalog#: S-2598 | $20.00 |  |
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